Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Base Information

• Chemical Name: Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester
• CAS No.: 88681-59-8
• Molecular Formula: C₈₆H₁₀₃N₁₁O₁₆S₂
• Molecular Weight: 1610.96

Synonyms:Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Chemical Property of Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Chemical Property:

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Technology Process of Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

There total 1 articles about Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteine Azide (88681-62-3) + o-Nitrobenzenesulfenylprolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-60-1) → Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-59-8)

Guidance literature:

With 1-ethyl-piperidine; In N,N-dimethyl-formamide; at 0 ℃; for 60h; Label VI used as hydrochloride;

DOI:10.1135/cccc19832862

Reference yield:

Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteinyl-prolyl-Nδ-benzyloxycarbonylornithine Benzyl Ester (88681-59-8) → <8-Ornithine, 9-desglycinamide> vasopressin (88480-55-1)

Guidance literature:

With sodium hydroxide; trifluorormethanesulfonic acid; methyl-phenyl-thioether; oxygen; Yield given; 1)Trifluoro acetic acid, 0 deg C, 30 min 2) Water 1 h;

DOI:10.1135/cccc19832862

upstream raw materials:

Benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)cysteinyl-tyrosyl-phenylalanyl-glutaminyl-asparaginyl-S-(2,4,6-trimethylbenzyl)cysteine Azide

o-Nitrobenzenesulfenylprolyl-N^δ-benzyloxycarbonylornithine Benzyl Ester

Downstream raw materials:

<8-Ornithine, 9-desglycinamide> vasopressin

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