C₂₅H₂₂O₂

Base Information

Chemical Name:C₂₅H₂₂O₂
CAS No.:1257517-87-5
Molecular Formula:C₂₅H₂₂O₂
Molecular Weight:354.448
Hs Code.:

C<sub>25</sub>H<sub>22</sub>O<sub>2</sub>

Synonyms:C₂₅H₂₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₂O₂

Chemical Property:

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Technology Process of C₂₅H₂₂O₂

There total 4 articles about C₂₅H₂₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1257517-86-4
C₂₅H₂₃IO₂

: 1257517-87-5
C₂₅H₂₂O₂

Guidance literature:: With palladium diacetate; triphenylphosphine; silver carbonate; In toluene; at 80 ℃; for 16h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/cmdc.201300175

Reference yield:

: 1257517-86-4
C₂₅H₂₃IO₂

: C₂₅H₂₂O₂

: 1257517-87-5
C₂₅H₂₂O₂

Guidance literature:: With palladium diacetate; triphenylphosphine; silver carbonate; In toluene; at 80 ℃; for 16h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c0ob00331j

Reference yield:

: 1257517-84-2
C₁₉H₁₈O₂

: 1257517-87-5
C₂₅H₂₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / toluene / 2 h / 0 - 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 0 - 20 °C

3: triphenylphosphine; silver carbonate; palladium diacetate / toluene / 16 h / 80 °C / Microwave irradiation; Inert atmosphere

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; palladium diacetate; triphenylphosphine; silver carbonate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In toluene; 2: |Mitsunobu Displacement;
DOI:10.1002/cmdc.201300175