Technology Process of C19H34Si
There total 8 articles about C19H34Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; toluene-4-sulfonic acid hydrazide;
In
1,4-dioxane;
at 120 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ja3093955
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; copper (I) trifluoromethane sulfonate toluene complex; potassium methanolate / dichloromethane; 1,4-dioxane / 48 h / 15 °C / Sealed tube; Inert atmosphere
2: toluene-4-sulfonic acid hydrazide; triethylamine / 1,4-dioxane / 1 h / 120 °C / Inert atmosphere
With
(R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; copper (I) trifluoromethane sulfonate toluene complex; potassium methanolate; triethylamine; toluene-4-sulfonic acid hydrazide;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/ja3093955
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,4-dioxane / 1 h / 60 °C / Sealed tube; Inert atmosphere
2: (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; copper (I) trifluoromethane sulfonate toluene complex; potassium methanolate / dichloromethane; 1,4-dioxane / 48 h / 15 °C / Sealed tube; Inert atmosphere
3: toluene-4-sulfonic acid hydrazide; triethylamine / 1,4-dioxane / 1 h / 120 °C / Inert atmosphere
With
(R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; copper (I) trifluoromethane sulfonate toluene complex; potassium methanolate; triethylamine; toluene-4-sulfonic acid hydrazide;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/ja3093955