sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

Base Information

Chemical Name:sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate
CAS No.:1607447-53-9
Molecular Formula:C₁₅H₁₉O₇S*Na
Molecular Weight:366.367
Hs Code.:

Synonyms:sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

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Chemical Property of sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

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Technology Process of sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

There total 8 articles about sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1607447-52-8
((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanethiol

: 1607447-53-9
sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium perchlorate; sodium hydrogencarbonate; potassium bromide; In water; acetonitrile; for 0.166667h;
DOI:10.1016/j.carres.2014.01.004

Reference yield:

: 1607447-50-6
(3aS,5S,6S,6aS)-6-(benzyloxy)-5-(iodomethyl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole

: 1607447-53-9
sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 1 h / 80 °C

2: sodium; methanol / 1 h

3: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium perchlorate / acetonitrile; water / 0.17 h

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium perchlorate; sodium; sodium hydrogencarbonate; potassium bromide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2014.01.004

Reference yield:

: 1607447-51-7
S-(((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl) ethanethioate

: 1607447-53-9
sodium ((3aS,5S,6S,6aS)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methanesulphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium; methanol / 1 h

2: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium perchlorate / acetonitrile; water / 0.17 h

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium perchlorate; sodium; sodium hydrogencarbonate; potassium bromide; In water; acetonitrile;
DOI:10.1016/j.carres.2014.01.004