methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:502698-54-6
Molecular Formula:C₈₆H₉₅NO₂₁
Molecular Weight:1478.69
Hs Code.:

methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Synonyms:methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 2 articles about methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 441777-56-6
methyl (2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: C₅₆H₅₄Cl₃NO₁₂

: 502698-54-6
methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; boron trifluoride diethyl etherate; In diethyl ether; at -78 - -10 ℃; for 3h;
DOI:10.1016/S0957-4166(02)00580-3

Reference yield: 11.0%

: 441777-56-6
methyl (2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: C₅₆H₅₄Cl₃NO₁₂

: 502698-54-6
methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-α-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: methyl (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1-4)-(2,3-di-O-benzoyl-β-L-rhamnopyranosyl)-(1-3)-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-(1-2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -78 - 4 ℃; for 7h;
DOI:10.1016/S0957-4166(02)00580-3