C₃₆H₃₃ClO₁₂S

Base Information

Chemical Name:C₃₆H₃₃ClO₁₂S
CAS No.:1334304-86-7
Molecular Formula:C₃₆H₃₃ClO₁₂S
Molecular Weight:725.17
Hs Code.:

C<sub>36</sub>H<sub>33</sub>ClO<sub>12</sub>S

Synonyms:C₃₆H₃₃ClO₁₂S

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Chemical Property of C₃₆H₃₃ClO₁₂S

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Technology Process of C₃₆H₃₃ClO₁₂S

There total 7 articles about C₃₆H₃₃ClO₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1334304-72-1
C₁₄H₁₄O₅S

: 2β-chloropodophyllotoxin

: 1334304-86-7
C₃₆H₃₃ClO₁₂S

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -15 - 20 ℃; stereoselective reaction;
DOI:10.1016/j.bmcl.2011.07.075

Reference yield:

: 62318-97-2
4-O-tetrahydropyran-2-ylpodophyllotoxin

: 1334304-86-7
C₃₆H₃₃ClO₁₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / -78 °C

1.2: 4 h / -78 °C

2.1: hydrogenchloride / tetrahydrofuran / 3 h / 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / -15 - 20 °C

With hydrogenchloride; boron trifluoride diethyl etherate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2011.07.075

Reference yield:

: 90-02-8
salicylaldehyde

: 1334304-86-7
C₃₆H₃₃ClO₁₂S

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 - 5 °C

2: sodium tetrahydroborate / methanol / 0 - 5 °C

3: boron trifluoride diethyl etherate / dichloromethane / -15 - 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; triethylamine; In methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.07.075