6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide

Base Information

• Chemical Name: 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide
• CAS No.: 188292-24-2
• Molecular Formula: C₁₀H₆Cl₂N₂O₂S
• Molecular Weight: 289.142
• Mol file: 188292-24-2.mol

Synonyms:6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide

Chemical Property of 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide

There total 1 articles about 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

2,3-bis(bromomethyl)-6,7-dichloroquinoxaline (3298-96-2) → 6,7-dichloro-2,3-dimethylquinoxaline (52736-71-7) + 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide (188292-24-2)

Guidance literature:

With rongalite; In N,N-dimethyl-formamide; at 0 ℃; for 7h; Yield given;

DOI:10.1039/a606764f

Reference yield: 54.0%

N-phenyl-maleimide (941-69-5) + 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide (188292-24-2) → 7,8-Dichloro-2-phenyl-3a,4,11,11a-tetrahydro-pyrrolo[3,4-b]phenazine-1,3-dione

Guidance literature:

In toluene; at 200 ℃;

DOI:10.1039/a606764f

Reference yield:

N-phenyl-maleimide (941-69-5) + 6,7-Dichloro-1,4-dihydro-2-oxa-3-thia-9,10-diaza-anthracene 3-oxide (188292-24-2) → C30H20Cl2N4O4 + C30H20Cl2N4O4

Guidance literature:

In toluene; at 200 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1039/a606764f

upstream raw materials:

2,3-bis(bromomethyl)-6,7-dichloroquinoxaline