C₃₇H₅₃N₅O₉

Base Information

Chemical Name:C₃₇H₅₃N₅O₉
CAS No.:1346444-99-2
Molecular Formula:C₃₇H₅₃N₅O₉
Molecular Weight:711.856
Hs Code.:

C<sub>37</sub>H<sub>53</sub>N<sub>5</sub>O<sub>9</sub>

Synonyms:C₃₇H₅₃N₅O₉

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Chemical Property of C₃₇H₅₃N₅O₉

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Technology Process of C₃₇H₅₃N₅O₉

There total 12 articles about C₃₇H₅₃N₅O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1356451-77-8
C₄₅H₅₉N₅O₁₀

: 1346444-99-2
C₃₇H₅₃N₅O₉

Guidance literature:: With acetic acid; zinc; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.062

Reference yield:

: C₃₇H₅₂N₄O₉

: 1346444-99-2
C₃₇H₅₃N₅O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / 1.5 h / 0 °C / Inert atmosphere

1.2: 0.05 h / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: 1.5 h / 0 °C / Inert atmosphere

4.1: pyridine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

5.1: acetic acid; zinc / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With pyridine; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.062

Reference yield:

: 1346445-07-5
C₂HF₃O₂*C₄₃H₅₇N₅O₉

: 1346444-99-2
C₃₇H₅₃N₅O₉

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: acetic acid; zinc / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

With pyridine; acetic acid; zinc; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.062