thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester

Base Information

• Chemical Name: thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester
• CAS No.: 952525-86-9
• Molecular Formula: C₂₄H₁₈ClN₄O₂PS
• Molecular Weight: 492.925
• Mol file: 952525-86-9.mol

Synonyms:thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester

Chemical Property of thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester

Chemical Property:

Purity/Quality:

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Technology Process of thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester

There total 1 articles about thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-4-hydroxyazobenzene (1689-82-3,20714-70-9,37790-28-6) → thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester (952525-86-9)

Guidance literature:

With trichlorothiophosphine; triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1002/chem.200204630

Reference yield: 85.0%

thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester (952525-86-9) + C32H23N3O2P2 (593249-34-4) → C56H41N8O4P3S

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1002/chem.200204630

Reference yield:

thiophosphorochloridic acid O,O'-bis-(4-phenylazo-phenyl) ester (952525-86-9) → C24H18N7O2PS

Guidance literature:

With sodium azide; In acetone; at 20 ℃; for 24h;

DOI:10.1002/chem.200204630

upstream raw materials:

trans-4-hydroxyazobenzene