<2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane

Base Information

• Chemical Name: <2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane
• CAS No.: 102724-88-9
• Molecular Formula: C₁₅H₂₂O
• Molecular Weight: 221.315

Synonyms:<2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane

Chemical Property of <2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane

Chemical Property:

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Technology Process of <2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane

There total 1 articles about <2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

<2'-(2-trideuteriomethyl-3-oxocyclohex-1-en-1-yl)ethenylidene>cyclohexane (102724-85-6) → <2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane (102724-88-9)

Guidance literature:

With sodium tetrahydroborate; cerium(III) chloride; In ethanol; for 2.5h; Ambient temperature;

DOI:10.1021/jo00366a025

Reference yield:

<2'-(3''-hydroxy-2''-(trideutriomethyl)cyclohex-1''-en-1''-yl)ethenylidene>cyclohexane (102724-88-9) → C15H19(2)H3O (102724-89-0) + C15H19(2)H3O (102724-90-3)

Guidance literature:

In 2,2,4-trimethylpentane; for 7.5h; Heating;

DOI:10.1021/jo00366a025

upstream raw materials:

<2'-(2-trideuteriomethyl-3-oxocyclohex-1-en-1-yl)ethenylidene>cyclohexane

Downstream raw materials:

C₁₅H₁₉⁽²⁾H₃O

C₁₅H₁₉⁽²⁾H₃O

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