Technology Process of C34H46N6O10
There total 9 articles about C34H46N6O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-{[bis({[tert-butoxycarbonyl]amino})methylidene]amino}benzoic acid;
With
2,4,6-trimethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.25h;
C16H23N3O5;
In
N,N-dimethyl-formamide;
for 2h;
DOI:10.1016/j.tet.2012.09.002
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonium acetate; acetic acid / methanol / 64 h / 60 °C
2.1: N,N-dimethyl-formamide / -10 - 20 °C
3.1: palladium on activated charcoal; hydrogen / ethanol / 50 °C / 750.08 Torr
4.1: 2,4,6-trimethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 20 °C
4.2: 2 h
With
2,4,6-trimethyl-pyridine; palladium on activated charcoal; ammonium acetate; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid;
In
methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.002
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl-formamide / -10 - 20 °C
2.1: palladium on activated charcoal; hydrogen / ethanol / 50 °C / 750.08 Torr
3.1: 2,4,6-trimethyl-pyridine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.25 h / 20 °C
3.2: 2 h
With
2,4,6-trimethyl-pyridine; palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.09.002
