(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

Base Information

Chemical Name:(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester
CAS No.:1026152-57-7
Molecular Formula:C₂₄H₃₀N₄O₂
Molecular Weight:406.528
Hs Code.:

Synonyms:(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

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Chemical Property of (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

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Technology Process of (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

There total 7 articles about (2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 922723-30-6
2-azido-1-benzyl-3-phenyl-propylamine

: 922723-33-9
N-succinimidyl carbonic acid cyclohexylmethyl ester

: 1026152-57-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

Guidance literature:: With triethanolamine; In water; toluene; at 20 ℃; for 1h;
DOI:10.1021/jm060754+

Reference yield:

: 6921-34-2
benzylmagnesium chloride

: 1026152-57-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: CuBr*DMS / tetrahydrofuran / 0.17 h / -78 °C

1.2: tetrahydrofuran / -78 - 20 °C

2.1: 91 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3.1: 64 percent / NaN₃ / dimethylformamide / 16 h / 60 °C

4.1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

5.1: triethanolamine / toluene; H₂O / 1 h / 20 °C

With sodium azide; copper(I) bromide dimethylsulfide complex; triethanolamine; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm060754+

Reference yield:

: 922722-32-5
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid tert-butyl ester

: 1026152-57-7
(2-azido-1-benzyl-3-phenyl-propyl)-carbamic acid cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

2: triethanolamine / toluene; H₂O / 1 h / 20 °C

With triethanolamine; trifluoroacetic acid; In dichloromethane; water; toluene;
DOI:10.1021/jm060754+