methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate
CAS No.:145889-33-4
Molecular Formula:C₂₅H₃₀N₂O₄
Molecular Weight:422.524
Hs Code.:

Synonyms:methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

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Chemical Property of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

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Technology Process of methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

There total 1 articles about methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 6-<(2-ethylbutyl)carbamoyl>indole

: 145889-33-4
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, 0 deg C, 1 h, 2.) DMF, RT, 18 h;
DOI:10.1021/jm00055a011

Reference yield: 69.0%

: 145889-33-4
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

: 145889-34-5
4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; for 18h; Ambient temperature;
DOI:10.1021/jm00055a011

Reference yield:

: 145889-33-4
methyl 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxybenzoate

: 4-<<6-<(2-ethylbutyl)carbamoyl>indol-1-yl>methyl>-3-methoxy-N-<(2-methylphenyl)sulfonyl>benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / aq. LiOH / tetrahydrofuran; methanol / 18 h / Ambient temperature

2: 73 percent / 4-(dimethylamino)pyridine (DMAP), 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide (WSCDI) / CH₂Cl₂ / 18 h / Ambient temperature

With dmap; lithium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00055a011