2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside
CAS No.:848647-25-6
Molecular Formula:C₅₇H₉₂O₁₃Si₄
Molecular Weight:1097.69
Hs Code.:

2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

Synonyms:2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

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Chemical Property of 2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

There total 3 articles about 2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 848647-23-4
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

: 302905-22-2
ethyl 3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2-thio-β-D-fructofuranoside

: 848647-25-6
2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 20 ℃; for 0.333333h;
DOI:10.1016/j.tetasy.2004.11.051

Reference yield:

: [2-((3aR,4R,5aR,8S,9aS,9bS)-2,2-Dibutyl-8-phenyl-hexahydro-1,3,5,7,9-pentaoxa-2-stanna-cyclopenta[a]naphthalen-4-yloxy)-ethyl]-trimethyl-silane

: 848647-25-6
2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.2 g / tetrabutylammonium iodide / acetonitrile / 2 h / 100 °C

2: 80 percent / DTBMP; DMTST; molecular sieves 4 Angstroem / CH₂Cl₂ / 0.33 h / 20 °C

With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetasy.2004.11.051

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 848647-25-6
2-(trimethylsilyl)ethyl [3-O-benzyl-6-O-tert-butyldimethylsilyl-1,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-fructofuranosyl]-(2->2)-4,6-O-benzylidene-3-O-p-methoxybenzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.2 g / tetrabutylammonium iodide / acetonitrile / 2 h / 100 °C

2: 80 percent / DTBMP; DMTST; molecular sieves 4 Angstroem / CH₂Cl₂ / 0.33 h / 20 °C

With 2,6-di-tert-butyl-4-methylpyridine; 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetasy.2004.11.051