Technology Process of C35H57NO6Si
There total 8 articles about C35H57NO6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C
2: 1H-imidazole / dichloromethane / 1 h / 0 °C
3: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C
With
1H-imidazole; sodium tetrahydroborate; triethylamine; calcium chloride;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C
2.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C
3.1: copper(II) sulfate / dichloromethane / 18 h / 20 °C
4.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 3 h / -78 °C
4.2: 60 h / -60 °C
5.1: hydrogenchloride / water; 1,4-dioxane; methanol / 1 h / 20 °C
6.1: triethylamine / water; 1,4-dioxane; methanol / 1 h / 0 - 20 °C
7.1: 1H-imidazole / dichloromethane / 1 h / 0 °C
8.1: sodium tetrahydroborate; calcium chloride / tetrahydrofuran / 3 h / 0 °C
With
1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; diisobutylaluminium hydride; copper(II) sulfate; triethylamine; calcium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water;
DOI:10.1016/j.tetlet.2013.01.110
