tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane

Base Information

Chemical Name:tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane
CAS No.:1264253-82-8
Molecular Formula:C₃₂H₅₄O₄Sn₂
Molecular Weight:740.198
Hs Code.:

Synonyms:tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane

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Chemical Property of tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane

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Technology Process of tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane

There total 1 articles about tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 260415-23-4
BrCH₂C₆H(OCH₃)3Sn(CH₃)3

: <2-(Hydroxymethyl)phenyl>tributyltin

: 1264253-82-8
tributyl(2-((3,4,5-trimethoxy-2-(trimethylstannyl)benzyloxy)methyl)phenyl)stannane

Guidance literature:: With NaH; In N,N-dimethyl-formamide; a soln. of HOCH2C6H4Sn(C4H9)3 added dropwise to a suspn. of NaH at 0°C, stirred for 10 min, a soln. of Br compd. added, stirred at 0°C for 20 min and at room temp. for 16 h; CH2Cl2 and H2O added, extd. with CH2Cl2, the combined ext. washed with brine, dried, evapd., flash-chromd. (silica gel, hexane/EtOAc); obtained as oil; elem. anal.;
DOI:10.1039/c0ob00500b