(S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

Base Information

Chemical Name:(S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide
CAS No.:182616-81-5
Molecular Formula:C₁₆H₁₉N₅O₃
Molecular Weight:329.359
Hs Code.:

Synonyms:(S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

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Chemical Property of (S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

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Technology Process of (S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

There total 2 articles about (S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 34897-85-3
o-azidobenzoyl chloride

: 85760-88-9
(S)-N,N-diethyl-5-oxopyrrolidine-2-carboxamide

: 182616-81-5
(S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h; 1.) 15 min;

Reference yield:

: 31162-13-7
2-azidobenzoic acid

: 182616-81-5
(S)-1-(2-Azido-benzoyl)-5-oxo-pyrrolidine-2-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / tetrahydrofuran / 2 h / 80 °C

2: 33 percent / 1.) LDA / tetrahydrofuran; hexane / 1 h / -78 °C / 1.) 15 min

With thionyl chloride; lithium diisopropyl amide; In tetrahydrofuran; hexane;