(S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester

Base Information

• Chemical Name: (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester
• CAS No.: 131550-31-7
• Molecular Formula: C₂₂H₂₉NO₇
• Molecular Weight: 419.475

Synonyms:(S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester

Chemical Property of (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester

Chemical Property:

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Technology Process of (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester

There total 1 articles about (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

Boc-Glu-OBn (30924-93-7) + magnesium monoallyl malonate (126690-67-3) → (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester (131550-31-7)

Guidance literature:

With 1,1'-carbonyldiimidazole; In acetonitrile; at 25 ℃;

DOI:10.1016/S0040-4039(00)97050-3

Reference yield: 66.0%

1-iodo-butane (542-69-8) + (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester (131550-31-7) → (S)-6-tert-Butoxycarbonylamino-2-butyl-3-oxo-heptanedioic acid 1-allyl ester 7-benzyl ester (131550-45-3)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

DOI:10.1016/S0040-4039(00)97050-3

Reference yield: 55.0%

1,4-Diiodobutane (628-21-7) + (S)-2-tert-Butoxycarbonylamino-5-oxo-heptanedioic acid 7-allyl ester 1-benzyl ester (131550-31-7) → 1-((S)-4-Benzyloxycarbonyl-4-tert-butoxycarbonylamino-butyryl)-cyclopentanecarboxylic acid allyl ester (131550-44-2)

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 18h;

DOI:10.1016/S0040-4039(00)97050-3

upstream raw materials:

Boc-Glu-OBn

magnesium monoallyl malonate

Downstream raw materials:

1-((S)-4-Benzyloxycarbonyl-4-tert-butoxycarbonylamino-butyryl)-cyclopentanecarboxylic acid allyl ester

(S)-6-tert-Butoxycarbonylamino-2-butyl-3-oxo-heptanedioic acid 1-allyl ester 7-benzyl ester

(S)-2-tert-Butoxycarbonylamino-5-oxo-decanoic acid benzyl ester

(S)-2-tert-Butoxycarbonylamino-5-cyclopentyl-5-oxo-pentanoic acid benzyl ester

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