2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

Base Information

Chemical Name:2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester
CAS No.:915779-98-5
Molecular Formula:C₁₆H₁₄F₅NO₄
Molecular Weight:379.283
Hs Code.:

2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-<i>tert</i>-butyl ester 2-pentafluorophenyl ester

Synonyms:2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

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Chemical Property of 2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

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Technology Process of 2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

There total 2 articles about 2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 90104-21-5
1-(tert-butoxycarbonyl)-2,3-dihydro-1H-pyrrole-2-carboxylic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 915779-98-5
2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃; for 4.5h;
DOI:10.1016/j.tet.2006.06.114

Reference yield:

: 83548-46-3
(S)-1-tert-butyl 2-methyl 2,3-dihydro-1H-pyrrole-1,2-dicarboxylate

: 915779-98-5
2,3-dihydro-pyrrole-1,2-dicarboxylic acid 1-tert-butyl ester 2-pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiOH / methanol; H₂O / 3 h / 20 °C

2: 65 percent / EDC / CH₂Cl₂ / 4.5 h / 20 °C

With lithium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dichloromethane; water;
DOI:10.1016/j.tet.2006.06.114