di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate

Base Information

Chemical Name:di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate
CAS No.:452339-70-7
Molecular Formula:C₂₂H₃₁NO₇
Molecular Weight:421.491
Hs Code.:
Mol file:452339-70-7.mol

Synonyms:di-(tert-butyl) 2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate

Suppliers and Price of di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

ChemScene
Di-(tert-butyl)2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate
5g
$ 900.00

ChemScene
Di-(tert-butyl)2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate
1g
$ 350.00

Total 2 raw suppliers

Chemical Property of di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Di-(tert-butyl)2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate

There total 5 articles about di-(tert-butyl)2-(2,2-diMethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliMinodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 102293-80-1
2-bromo-1-(2,2-dimethyl-4H-benzo[d][1,3]dioxin-6-yl)ethanone

: 452339-70-7
di-(tert-butyl) 2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 - 25 ℃; for 6h; Inert atmosphere;

Reference yield:

: 52113-69-6
6-bromo-2,2-dimethyl-4H-benzo[1,3]dioxine

: 452339-70-7
di-(tert-butyl) 2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / -75 - -70 °C

1.2: -75 - -70 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -75 - -70 °C

2.2: -75 - -70 °C

3.1: caesium carbonate / acetonitrile / 6 h / 20 - 25 °C / Inert atmosphere

With n-butyllithium; sodium hexamethyldisilazane; caesium carbonate; In tetrahydrofuran; acetonitrile;

Reference yield:

: 2316-64-5
5-bromo-2-hydroxybenzyl alcohol

: 452339-70-7
di-(tert-butyl) 2-(2,2-dimethyl-4H-1,3-benzodioxin-6-yl)-2-oxoethyliminodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / tetrahydrofuran / 1 h / 0 - 30 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 1 h / -75 - -70 °C

2.2: -75 - -70 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -75 - -70 °C

3.2: -75 - -70 °C

4.1: caesium carbonate / acetonitrile / 6 h / 20 - 25 °C / Inert atmosphere

With aluminum (III) chloride; n-butyllithium; sodium hexamethyldisilazane; caesium carbonate; In tetrahydrofuran; acetonitrile;