N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

Base Information

Chemical Name:N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide
CAS No.:1407182-20-0
Molecular Formula:C₃₁H₄₈N₂O
Molecular Weight:464.735
Hs Code.:

Synonyms:N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

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Technology Process of N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

There total 2 articles about N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1407182-19-7
N-(2-(2,6-diisobutylphenylamino)ethyl)-2,6-diisobutylbenzenamine

: 2258-42-6
formyl acetic anhydride

: 1407182-20-0
N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

Guidance literature:: In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2cc36329a

Reference yield:

: 957761-25-0
2,6-diisobutylaniline

: 1407182-20-0
N-(2,6-diisobutylphenyl)-N-(2-(2,6-diisobutylphenylamino)ethyl)formamide

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid; ethanol / water / 24 h / 70 °C / Inert atmosphere

2: sodium cyanoborohydride / diethyl ether; ethanol; acetic acid / 4 h / 20 °C

3: dichloromethane / 2 h / 20 °C / Inert atmosphere

With formic acid; ethanol; sodium cyanoborohydride; In diethyl ether; ethanol; dichloromethane; water; acetic acid;
DOI:10.1039/c2cc36329a