tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

Base Information

Chemical Name:tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate
CAS No.:1263324-74-8
Molecular Formula:C₁₆H₂₂N₂O₃
Molecular Weight:290.362
Hs Code.:

Synonyms:tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

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Chemical Property of tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

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Technology Process of tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

There total 1 articles about tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 400819-84-3
1,1-dimethylethyl 1-methyl-2-(1-methylethylidene)hydrazinecarboxylate

: 1263324-74-8
tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

Guidance literature:: 1,1-dimethylethyl 1-methyl-2-(1-methylethylidene)hydrazinecarboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

benzoic acid methyl ester; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.057

Reference yield: 100.0%

: 1263324-74-8
tert-butyl 1-methyl-2-(4-oxo-4-phenylbutan-2-ylidene)hydrazinecarboxylate

: 10250-58-5
1,3-dimethyl-5-phenyl-1H-pyrazole

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.057