methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

Base Information

Chemical Name:methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate
CAS No.:904681-98-7
Molecular Formula:C₁₈H₁₉NO₅
Molecular Weight:329.353
Hs Code.:

Synonyms:methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

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Technology Process of methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

There total 1 articles about methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 52480-43-0
4,5-dimethyl-2-formylfuran

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 904681-98-7
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

Guidance literature:: With potassium tert-butylate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.200600192

Reference yield:

: 904681-98-7
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

: 904682-03-7
methyl (2R)-(-)-2-benzyloxycarbonylamino-3-(4,5-dimethylfuran-2-yl)propanoate

: methyl (2S)-2-benzyloxycarbonylamino-3-(4,5-dimethylfuran-2-yl)propanoate

Guidance literature:: With hydrogen; di(norbornadiene)rhodium(I) tetrafluoroborate; In methanol; toluene; at 20 ℃; for 64h; under 3750.38 Torr; Title compound not separated from byproducts.;
DOI:10.1002/chem.200600192

Reference yield:

: 904681-98-7
methyl (2Z)-2-{[(benzyloxy)carbonyl]amino}-3-(4,5-dimethyl-2-furyl)acrylate

: 904682-19-5
(-)-benzyl (1R)-[2-(4,5-dimethyl-2-furyl)-1-(hydroxymethyl)ethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: MandyPhos(OMe); H₂ / [Rh(nbd)2]BF₄ / methanol; toluene / 64 h / 20 °C / 3750.38 Torr

2: 60 percent / DIBALH / tetrahydrofuran; hexane / -78 - 20 °C

With hydrogen; diisobutylaluminium hydride; di(norbornadiene)rhodium(I) tetrafluoroborate; In tetrahydrofuran; methanol; hexane; toluene;
DOI:10.1002/chem.200600192