phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside
CAS No.:945631-68-5
Molecular Formula:C₂₆H₂₅NO₉S
Molecular Weight:527.552
Hs Code.:

Synonyms:phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

There total 7 articles about phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64952-23-4
3-hydroxy-2-(1-methoxy-2-oxoethoxy)propanal

: 945631-68-5
phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: sodium methoxide / methanol / 8 h / -10 - 20 °C

2: 12 g / hydrogen / Raney nickel / ethanol / 24 h / 2585.81 Torr

3: triethylamine / dimethylformamide / 12 h / 100 °C

4: 2.2 g / pyridine / 12 h / 20 °C

5: HClO₄ / 24 h / 20 °C

6: 2.0 g / BF₃*OEt₂ / CH₂Cl₂

With pyridine; perchloric acid; boron trifluoride diethyl etherate; hydrogen; sodium methylate; triethylamine; nickel; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Henry reaction;
DOI:10.1021/jo070473p

Reference yield:

: 37073-79-3,409095-60-9
Methyl-3-nitro-3-desoxy-α-D-mannopyranosid

: 945631-68-5
phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 12 g / hydrogen / Raney nickel / ethanol / 24 h / 2585.81 Torr

2: triethylamine / dimethylformamide / 12 h / 100 °C

3: 2.2 g / pyridine / 12 h / 20 °C

4: HClO₄ / 24 h / 20 °C

5: 2.0 g / BF₃*OEt₂ / CH₂Cl₂

With pyridine; perchloric acid; boron trifluoride diethyl etherate; hydrogen; triethylamine; nickel; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo070473p

Reference yield:

: 97-30-3
methyl-alpha-D-glucopyranoside

: 945631-68-5
phenyl 2,4,6-tri-O-acetyl-3-deoxy-3-phthalimido-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: sodium metaperiodate / H₂O / 1.5 h

2: sodium methoxide / methanol / 8 h / -10 - 20 °C

3: 12 g / hydrogen / Raney nickel / ethanol / 24 h / 2585.81 Torr

4: triethylamine / dimethylformamide / 12 h / 100 °C

5: 2.2 g / pyridine / 12 h / 20 °C

6: HClO₄ / 24 h / 20 °C

7: 2.0 g / BF₃*OEt₂ / CH₂Cl₂

With pyridine; sodium periodate; perchloric acid; boron trifluoride diethyl etherate; hydrogen; sodium methylate; triethylamine; nickel; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 2: Henry reaction;
DOI:10.1021/jo070473p