10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid

Base Information

• Chemical Name: 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid
• CAS No.: 1313371-01-5
• Molecular Formula: C₁₈H₁₃ClN₂O₄
• Molecular Weight: 356.765

Synonyms:10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid

Chemical Property of 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid

Chemical Property:

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Technology Process of 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid

There total 2 articles about 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

tetrahydrofuran-2,4-dione (4971-56-6) + 4-chlorobenzaldehyde (104-88-1) + 3,4-diaminobenzoic acid (619-05-6) → 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid (1313371-01-5)

Guidance literature:

tetrahydrofuran-2,4-dione; 3,4-diaminobenzoic acid; With acetic acid; In water; for 0.5h;

4-chlorobenzaldehyde; In water; at 110 ℃; for 0.2h; regioselective reaction; Microwave irradiation;

DOI:10.1016/j.tet.2011.05.002

Reference yield: 45.0%

tetrahydrofuran-2,4-dione (4971-56-6) + 4-chlorobenzaldehyde (104-88-1) + 3,4-diaminobenzoic acid (619-05-6) → 10-(4-chlorophenyl)-1-oxo-3,4,9,10-tetrahydro-1H-2-oxa-4,9-diaza-benzo[f]azulene-6-carboxylic acid (1313371-01-5) + 2-(4-chlorophenyl)-1H-benzimidazole-5-carboxylic acid (174422-14-1)

Guidance literature:

In benzene; at 90 ℃; for 0.266667h; Microwave irradiation;

DOI:10.1016/j.tet.2011.05.002

upstream raw materials:

tetrahydrofuran-2,4-dione

4-chlorobenzaldehyde

3,4-diaminobenzoic acid

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