(1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

Base Information

Chemical Name:(1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate
CAS No.:1174527-55-9
Molecular Formula:C₁₅H₁₆ClNO
Molecular Weight:261.751
Hs Code.:

Synonyms:(1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

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Chemical Property of (1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

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Technology Process of (1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

There total 1 articles about (1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: (MP,S)-1-[2-(2-chlorophenyl)-1-cyclohexenyl]ethyl carbamate

: 1174527-55-9
(1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

Guidance literature:: With carbon tetrabromide; triethylamine; triphenylphosphine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.004

Reference yield: 92.0%

: 1174527-55-9
(1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate

: 1174527-56-0
(R)-1-(2-chlorophenyl)-2-ethylidene-1-methylaminocyclohexane

Guidance literature:: (1R,2E)-1-(2-chlorophenyl)-2-ethylidenecyclohexyl isocyanate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Reflux;

With water; sodium hydroxide; In tetrahydrofuran; at 90 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2009.05.004