{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

Base Information

Chemical Name:{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol
CAS No.:181589-29-7
Molecular Formula:C₂₁H₃₆N₂O₂
Molecular Weight:348.529
Hs Code.:

Synonyms:{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

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Chemical Property of {(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

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Technology Process of {(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

There total 4 articles about {(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 181589-29-7
{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / p-TsOH, molecular sieves / toluene / 3 h

2: 83 percent / LDA, TMEDA; LiALH₄ / tetrahydrofuran; diethyl ether; hexane / 1.) -100 deg C to r.t.; r.t., 15 h, 2.) r.t., 3 h

With lithium aluminium tetrahydride; molecular sieve; N,N,N,N,-tetramethylethylenediamine; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; toluene;

Reference yield:

: 42134-55-4,114096-03-6,132350-24-4
3-cyclohexyl-2-propen-1-ol

: 181589-29-7
{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / DMAP, molecular sieves 4 Angstroem / toluene / 48 h / Heating

2: 87 percent / p-TsOH, molecular sieves / toluene / 3 h

3: 83 percent / LDA, TMEDA; LiALH₄ / tetrahydrofuran; diethyl ether; hexane / 1.) -100 deg C to r.t.; r.t., 15 h, 2.) r.t., 3 h

With dmap; lithium aluminium tetrahydride; molecular sieve; N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; toluene;

Reference yield:

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 181589-29-7
{(R)-1-((S)-1-Cyclohexyl-allyl)-2-[(E)-(S)-2-methoxymethyl-pyrrolidin-1-ylimino]-cyclopentyl}-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / DMAP, molecular sieves 4 Angstroem / toluene / 48 h / Heating

2: 87 percent / p-TsOH, molecular sieves / toluene / 3 h

3: 83 percent / LDA, TMEDA; LiALH₄ / tetrahydrofuran; diethyl ether; hexane / 1.) -100 deg C to r.t.; r.t., 15 h, 2.) r.t., 3 h

With dmap; lithium aluminium tetrahydride; molecular sieve; N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; toluene;