C₁₂H₁₈ClFSi

Base Information

• Chemical Name: C₁₂H₁₈ClFSi
• CAS No.: 1151691-05-2
• Molecular Formula: C₁₂H₁₈ClFSi
• Molecular Weight: 244.812

Synonyms:C₁₂H₁₈ClFSi

Chemical Property of C₁₂H₁₈ClFSi

Chemical Property:

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Technology Process of C₁₂H₁₈ClFSi

There total 1 articles about C₁₂H₁₈ClFSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-fluorobromobenzene (1073-06-9) → C12H18ClFSi (1151691-05-2)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium / hexane / Schlenk technique; Inert atmosphere

2: diethyl ether / 3 h / -78 °C / Schlenk technique; Inert atmosphere

With n-butyllithium; In diethyl ether; hexane;

DOI:10.1021/jacs.7b08055

Reference yield: 66.0%

2-hydroxybromobenzene (95-56-7) + C12H18ClFSi (1151691-05-2) → 2-bromophenyl (3-fluorophenyl)diisopropylsilyl ether (1116155-98-6)

Guidance literature:

With 1H-imidazole; In dichloromethane; at 40 ℃; for 12h; Inert atmosphere;

DOI:10.1002/anie.200804146

Reference yield:

C12H18ClFSi (1151691-05-2) + (2,6-diisopropylphenyl)oxy-1,2-dichloroethene → diisopropyl-(3-fluorophenyl)-(2,6-diisopropylphenoxyethynyl)silane

Guidance literature:

(2,6-diisopropylphenyl)oxy-1,2-dichloroethene; With n-butyllithium; In diethyl ether; hexane; at -78 - -40 ℃; for 4h; Schlenk technique; Inert atmosphere;

C₁₂H₁₈ClFSi; With N,N,N,N,N,N-hexamethylphosphoric triamide; In diethyl ether; hexane; at -78 - 20 ℃; for 14h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jacs.7b08055

upstream raw materials:

3-fluorobromobenzene

Downstream raw materials:

2-bromophenyl (3-fluorophenyl)diisopropylsilyl ether

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