methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside

Base Information

• Chemical Name: methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside
• CAS No.: 1350973-23-7
• Molecular Formula: C₃₉H₄₀O₆
• Molecular Weight: 605.735

Synonyms:methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside

Chemical Property of methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside

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Technology Process of methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside

There total 1 articles about methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(S)-benzyl-α-d1-4-methylbenzenesulfonate (61866-19-1) + methyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-α-D-glucopyranoside (291314-27-7) → methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside (1350973-23-7)

Guidance literature:

With sodium hydride; In dichloromethane; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c1ob06056b

Reference yield: 95.0%

methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-4-O-(2-naphthylmethyl)-α-D-glucopyranoside (1350973-23-7) → methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-α-D-glucopyranoside (851895-47-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 4h;

DOI:10.1039/c1ob06056b

upstream raw materials:

(S)-benzyl-α-d1-4-methylbenzenesulfonate

methyl 2,3-di-O-benzyl-4-O-(2-naphthyl)methyl-α-D-glucopyranoside

Downstream raw materials:

methyl 6-O-(R)-benzyl-α-d1-2,3-di-O-benzyl-α-D-glucopyranoside

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