2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Base Information

Chemical Name:2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate
CAS No.:1403363-71-2
Molecular Formula:C₂₁H₁₇ClFN₂S₂*C₂₄H₂₀B
Molecular Weight:735.197
Hs Code.:

Synonyms:2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Suppliers and Price of 2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

There total 3 articles about 2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 938079-65-3
5-fluoro-N,2-dimethyl-1,3-benzothiazolium iodide

: 1403363-45-0
5-chloro-3-methyl-2-(4-(N-phenylacetamido)buta-1,3-dien-1-yl)benzothiazol-3-ium iodide

: 143-66-8
sodium tetraphenyl borate

: 1403363-71-2
2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Guidance literature:: 5-fluoro-N,2-dimethyl-1,3-benzothiazolium iodide; 5-chloro-3-methyl-2-(4-(N-phenylacetamido)buta-1,3-dien-1-yl)benzothiazol-3-ium iodide; With triethylamine; In ethanol; for 1h; Reflux;

sodium tetraphenyl borate; for 1h; Reflux;
DOI:10.1016/j.dyepig.2012.07.007

Reference yield:

: 399-75-7
5-fluoro-2-methyl-1,3-benzothiazole

: 1403363-71-2
2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide

2.1: triethylamine / ethanol / 1 h / Reflux

2.2: 1 h / Reflux

With triethylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2012.07.007

Reference yield:

: 23769-16-6,28140-60-5,50328-50-2,58467-94-0,125367-88-6
phenyl[3-phenylaminoprop-2-en-1-ylidene]ammonium chloride

: 1403363-71-2
2-(5-(5-chloro-3-methylbenzothiazol-2(3H)-ylidene)penta-1,3-dien-1-yl)-5-fluoro-3-methylbenzothiazol-3-ium tetraphenylborate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / 2 h / Reflux

2.1: triethylamine / ethanol / 1 h / Reflux

2.2: 1 h / Reflux

With acetic acid; triethylamine; In ethanol;
DOI:10.1016/j.dyepig.2012.07.007