Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

Base Information

Chemical Name:Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride
CAS No.:1147834-45-4
Molecular Formula:C₆₅H₈₀N₁₆O₁₉*ClH
Molecular Weight:1425.91
Hs Code.:

Synonyms:Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

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Chemical Property of Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

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Technology Process of Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

There total 1 articles about Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1147835-24-2
Boc-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn

: 1147834-45-4
Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1h; under 750.075 Torr; Inert atmosphere;
DOI:10.1016/j.ejmech.2008.09.036

Reference yield: 71.4%

: 1147834-45-4
Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

: 41164-36-7
2-<(17β-Hydroxyestra-1,3,5(10)-trien-3-yl)oxy>acetic Acid

: 1147834-60-3
estradiol-3-O-acetyl-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn

Guidance literature:: 2-<(17β-Hydroxyestra-1,3,5(10)-trien-3-yl)oxy>acetic Acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.5h; under 750.075 Torr; Inert atmosphere;

Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride; With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃; under 750.075 Torr; pH=8.5; Inert atmosphere;
DOI:10.1016/j.ejmech.2008.09.036

Reference yield: 65.3%

: 1147834-45-4
Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride

: 7698-93-3
Estradiol-17-hemisuccinate

: 1147834-79-4
estradiol-17β-O-4-oxobutanoyl-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn

Guidance literature:: Estradiol-17-hemisuccinate; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.5h; under 750.075 Torr; Inert atmosphere;

Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-Arg(Nω-NO2)-Gly-Asp(OBn)-Ser(Bn)-OBn hydrochloride; With 4-methyl-morpholine; In tetrahydrofuran; at 0 ℃; under 750.075 Torr; pH=8.5; Inert atmosphere;
DOI:10.1016/j.ejmech.2008.09.036