NBu₄[PdBr(C₆F₅)(acetylacetonato)]

Base Information

• Chemical Name: NBu₄[PdBr(C₆F₅)(acetylacetonato)]
• CAS No.: 915377-71-8
• Molecular Formula: C₁₁H₇BrF₅O₂Pd*C₁₆H₃₆N
• Molecular Weight: 694.96

Synonyms:NBu₄[PdBr(C₆F₅)(acetylacetonato)]

Chemical Property of NBu₄[PdBr(C₆F₅)(acetylacetonato)]

Chemical Property:

Purity/Quality:

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Technology Process of NBu₄[PdBr(C₆F₅)(acetylacetonato)]

There total 1 articles about NBu₄[PdBr(C₆F₅)(acetylacetonato)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(NBu4)2{Pd2(μ-Br)2(C6F5)2Br2} + thallium(I) 2,4-pentanedionate → NBu4[PdBr(C6F5)(acetylacetonato)] (915377-71-8)

Guidance literature:

In dichloromethane; (N2); Tl compd. added to a soln. of Pd complex, stirred in the absence of light for 1.5 h at room temp.; filtered, evapd., Et2O added, crystd. on cooling, filtered, washed (Et2O), air-dried; elem. anal.;

DOI:10.1021/om060622e

Reference yield: 61.0%

NBu4[PdBr(C6F5)(acetylacetonato)] (915377-71-8) + acetonitrile (75-05-8,26809-02-9) → [Pd(C6F5)(acetylacetonato)(acetonitrile)] (915377-60-5)

Guidance literature:

With silver tetrafluoroborate; In acetonitrile; (N2); Pd complex added to a soln. of AgBF4, stirred in the absence of light for 1 h at room temp.; filtered, evapd., extd. (Et2O), MeCN added, concd., n-hexane added, crystd. at -30°C, filtered, washed (cold Et2O), air-dried; elem. anal.;

DOI:10.1021/om060622e

Downstream raw materials:

[Pd(C₆F₅)(acetylacetonato)(acetonitrile)]

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