((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

Base Information

Chemical Name:((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2
CAS No.:106040-32-8
Molecular Formula:C₄₄H₈₂O₂Si₄Ta₂
Molecular Weight:1117.37
Hs Code.:

((CH<sub>3</sub>)3SiCH<sub>2</sub>)2Ta(CSi(CH<sub>3</sub>)3)2Ta(OC<sub>6</sub>H<sub>3</sub>(C<sub>4</sub>H<sub>9</sub>)2)2

Synonyms:((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

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Chemical Property of ((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

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Technology Process of ((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

There total 1 articles about ((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 128-39-2
2,6-di-tert-butylphenol

: 34844-62-7,107201-09-2
{(Me3SiCH2)Ta(μ-CSiMe3)2Ta(CH2SiMe3)2}

: 106040-32-8
((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

Guidance literature:: In toluene; mixt. of Ta-deriv. with 2 equiv of phenol heated at 100°C for 24 h under N2; soln. evapd. under vacuum, residue taken up in hexane, filtered, and cooled to -15°C; elem. anal.;

Reference yield: 5.0%

: 106040-32-8
((CH₃)3SiCH₂)2Ta(CSi(CH₃)3)2Ta(OC₆H₃(C₄H₉)2)2

: 75-76-3
tetramethylsilane

: 83830-98-2
Ta(OC₆H₃-t-BuCMe₂CH₂)2(CH₂SiMe₃)

: 128-39-2
2,6-di-tert-butylphenol

Guidance literature:: In ⁽²⁾H₈-toluene; heated at 150°C in a sealed NMR tube for 5-10 h; not isolated ((1)H NMR data); yield of the cyclometallated complex increases when thermolysis is carried out in the presence of 2 or more equiv of 2,6-t-Bu2C6H3OH;