(-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

Base Information

Chemical Name:(-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane
CAS No.:138517-58-5
Molecular Formula:C₆₁H₅₁NO₄P₂
Molecular Weight:924.028
Hs Code.:

Synonyms:(-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

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Chemical Property of (-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

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Technology Process of (-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

There total 2 articles about (-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.2%

: 17261-28-8
ortho-diphenylphosphinobenzoic acid

: 143668-56-8
bis N-<(1R)-1-hydroxyphenylethan-2-yl> benzylamine

: 138517-58-5
(-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 36h; Ambient temperature;
DOI:10.1021/ja00050a013

Reference yield:

: 100-46-9
benzylamine

: 138517-58-5
(-)-3-aza-3-benzyl-1(R),5(R)-dihydroxy-1,5-bis-O-<2'-(diphenylphosphino)benzoyl>-1,5-diphenylpentane

Guidance literature:: Multi-step reaction with 2 steps

1: 78.1 percent / 13 h / 120 °C

2: 30.2 percent / DCC, DMAP / CH₂Cl₂ / 36 h / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ja00050a013