3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

Base Information

Chemical Name:3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al
CAS No.:484068-08-8
Molecular Formula:C₂₂H₂₈O₃
Molecular Weight:340.463
Hs Code.:

Synonyms:3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

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Chemical Property of 3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

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Technology Process of 3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

There total 11 articles about 3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-3-(4-Methoxy-benzyloxy)-3-phenethyl-hexan-1-ol

: 484068-08-8
3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 25 ℃;
DOI:10.1021/ja028497v

Reference yield:

: 591-50-4
iodobenzene

: 484068-08-8
3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / Pd(OAc)2; P(o-Tol)3; Et₃N / toluene / Heating

2: 99 percent / H₂; pyridine / Pd/C / methanol / 25 °C / 760.05 Torr

3: Dess-Martin periodinane / CH₂Cl₂ / 25 °C

4: tetrahydrofuran / Heating

5: (Ph₃P)3RhCl / tetrahydrofuran

6: 3N aq. NaOH; 30percent aq. H₂O₂ / 25 °C

7: Dess-Martin periodinane / CH₂Cl₂ / 25 °C

With pyridine; palladium diacetate; sodium hydroxide; Wilkinson's catalyst; hydrogen; Dess-Martin periodane; triethylamine; tris-(o-tolyl)phosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Heck arylation / 3: Dess-Martin oxidation / 4: Wittig olefination / 7: Dess-Martin oxidation;
DOI:10.1021/ja028497v

Reference yield:

: 19265-24-8
1-chloropentane-2-one

: 484068-08-8
3-(4-methoxybenzyloxy)-3-phenylethylhexan-1-al

Guidance literature:: Multi-step reaction with 10 steps

1: tetrahydrofuran / 0 °C

2: aq. NaOH / diethyl ether / 25 °C

3: 69 percent / Pd₂(dba)3*CHCl₃; (S,S)-N,N'-bis(o-PPh₂C₆H₄CO)-1,2-cyclohexylenediamine; Et₃B

4: 92 percent / Pd(OAc)2; P(o-Tol)3; Et₃N / toluene / Heating

5: 99 percent / H₂; pyridine / Pd/C / methanol / 25 °C / 760.05 Torr

6: Dess-Martin periodinane / CH₂Cl₂ / 25 °C

7: tetrahydrofuran / Heating

8: (Ph₃P)3RhCl / tetrahydrofuran

9: 3N aq. NaOH; 30percent aq. H₂O₂ / 25 °C

10: Dess-Martin periodinane / CH₂Cl₂ / 25 °C

With pyridine; trans-1,2-(1S,2S)-1,2-diaminocyclohexane-N,N’-bis(2’-diphenylphosphinobenzoyl); tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium diacetate; sodium hydroxide; Wilkinson's catalyst; triethyl borane; hydrogen; Dess-Martin periodane; triethylamine; tris-(o-tolyl)phosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 4: Heck arylation / 6: Dess-Martin oxidation / 7: Wittig olefination / 10: Dess-Martin oxidation;
DOI:10.1021/ja028497v