C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾
CAS No.:1408317-75-8
Molecular Formula:C₃₂H₄₂NO₁₈S*Na
Molecular Weight:783.737
Hs Code.:

C<sub>32</sub>H<sub>42</sub>NO<sub>18</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

There total 6 articles about C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1408317-71-4
C₃₂H₄₃NO₁₅

: 1408317-75-8
C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: With sulfur trioxide-N,N-dimethylformamide complex; In N,N-dimethyl-formamide; at 55 ℃; for 12h;
DOI:10.1002/chem.201200887

Reference yield:

: 1402076-31-6
C₂₄H₃₈O₇Si

: 1408317-75-8
C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -40 - -20 °C / Molecular sieve

2: hydrogen fluoride / water; acetonitrile / 2 h / 20 °C

3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Inert atmosphere; Reflux

4: sulfur trioxide-N,N-dimethylformamide complex / N,N-dimethyl-formamide / 12 h / 55 °C

With sulfur trioxide-N,N-dimethylformamide complex; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; hydrogen fluoride; tri-n-butyl-tin hydride; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201200887

Reference yield:

: 161545-19-3
3,4,6-tri-O-acetyl-2-deoxy-2-trichloroacetamido-α/β-D-glucopyranose trichloroacetimidate

: 1408317-75-8
C₃₂H₄₂NO₁₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / dichloromethane / 4 h / -40 - -20 °C / Molecular sieve

2: hydrogen fluoride / water; acetonitrile / 2 h / 20 °C

3: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.5 h / Inert atmosphere; Reflux

4: sulfur trioxide-N,N-dimethylformamide complex / N,N-dimethyl-formamide / 12 h / 55 °C

With sulfur trioxide-N,N-dimethylformamide complex; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; hydrogen fluoride; tri-n-butyl-tin hydride; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1002/chem.201200887