<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Base Information

Chemical Name:<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone
CAS No.:138704-21-9
Molecular Formula:C₂₅H₂₅N₃O₇
Molecular Weight:479.489
Hs Code.:

Synonyms:<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Suppliers and Price of <2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

There total 9 articles about <2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 138704-20-8
<6S,4R(1'S,2'R)>-6-hydroxy-4-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-N-tryptophyl-2-piperidone-2'-6-anhydro

: 138704-21-9
<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Guidance literature:: With water; acetic acid; for 3h; Heating;
DOI:10.1016/S0040-4039(00)92154-3

Reference yield:

: 88901-92-2
methyl 4,6-O-benzylidene-3-C-(carbomethoxy-methylene)-2,3-didesoxy-α-D-ribo-hexapyranoside

: 138704-21-9
<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / hydrogen / 10percent Pd-C / methanol / 12 h

2: 80 percent / pyridine / 20 deg C, 24 h, then 70 deg C, 1 h

3: 87 percent / acetic acid, water / 12 h / Heating

4: 85 percent / acetic acid / benzene / 2 h / Heating

5: 90 percent / 30percent aq. acetic acid / 3 h / Heating

With pyridine; water; hydrogen; acetic acid; palladium on activated charcoal; In methanol; benzene;
DOI:10.1016/S0040-4020(01)80014-4

Reference yield:

: 134747-17-4
methyl 3-C-(carboxymethylene)-2,3-didesoxy-α-D-ribo-hexapyranoside-2',4-γ-lactone

: 138704-21-9
<2R(1'S,2'R),(12bR,12bS)>-2-<1'-(3'-O-p-nitrobenzoyl-1',2',3'-trihydroxypropyl)>-indolo<2,3-a>-4-quinolizidinone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridine / 20 deg C, 24 h, then 70 deg C, 1 h

2: 87 percent / acetic acid, water / 12 h / Heating

3: 85 percent / acetic acid / benzene / 2 h / Heating

4: 90 percent / 30percent aq. acetic acid / 3 h / Heating

With pyridine; water; acetic acid; In benzene;
DOI:10.1016/S0040-4020(01)80014-4