2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

Base Information

Chemical Name:2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole
CAS No.:865855-40-9
Molecular Formula:C₄₄H₅₅N₃O₄
Molecular Weight:689.938
Hs Code.:

Synonyms:2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

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Chemical Property of 2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

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Technology Process of 2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

There total 7 articles about 2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 16200-52-5
3,4-diethyl-1H-pyrrole

: 406483-36-1
benzyl 5-acetoxymethyl-4-n-butyl-3-methylpyrrole-2-carboxylate

: 865855-40-9
2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

Guidance literature:: In ethanol; acetic acid; for 18h; Heating;
DOI:10.1002/chem.200601644

Reference yield:

: 1540-36-9
3-butylpentane-2,4-dione

: 865855-40-9
2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium nitrite / acetic acid; H₂O / 20 °C

1.2: 85 percent / zinc; sodium acetate / acetic acid; H₂O / 80 - 90 °C

2.1: 87 percent / lead tetraacetate / acetic acid / 2 h / 20 °C

3.1: 72 percent / acetic acid; ethanol / 18 h / Heating

With lead(IV) acetate; sodium nitrite; In ethanol; water; acetic acid;
DOI:10.1002/chem.200601644

Reference yield:

: 93341-72-1
benzyloxycarbonyl-2 dimethyl-3,5 butyl-4 pyrrole

: 865855-40-9
2,5-bis((5-benzyloxycarbonyl-3-n-butyl-4-methyl-2-pyrrolyl)methyl)-3,4-diethyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / lead tetraacetate / acetic acid / 2 h / 20 °C

2: 72 percent / acetic acid; ethanol / 18 h / Heating

With lead(IV) acetate; In ethanol; acetic acid;
DOI:10.1002/chem.200601644