N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

Base Information

Chemical Name:N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine
CAS No.:119139-06-9
Molecular Formula:C₁₄H₁₇N₅O₃
Molecular Weight:303.321
Hs Code.:

Synonyms:N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

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Chemical Property of N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

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Technology Process of N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

There total 1 articles about N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1-benzyloxy-9-(methoxymethyl)adenine perchlorate

: 119139-06-9
N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

Guidance literature:: With water; at 40 ℃; for 5h; pH 9.2;
DOI:10.3987/COM-88-4519

Reference yield: 74.0%

: 119139-06-9
N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

: 51806-20-3
1,1-diethoxy-2-iodoethane

: 119139-07-0
N'-benzyloxy-5--1-(methoxymethyl)-1H-imidazole-4-carboxamidine

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 27h;
DOI:10.3987/COM-88-4519

Reference yield:

: 119139-06-9
N'-benzyloxy-5-formamido-1-(methoxymethyl)-1H-imidazole-4-carboxamidine

: N'-benzyloxy-5-(2,2-diethoxyethylamino)-1-(methoxymethyl)-1H-imidazole-4-carboxamidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / K₂CO₃, 18-crown-6 / dimethylformamide / 27 h / 30 °C

2: 95 percent / 1N NaOH / 3 h

With sodium hydroxide; 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.3987/COM-88-4519