Technology Process of C51H49N7O7
There total 5 articles about C51H49N7O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C57H63N7O7Si;
With
hydrogen fluoride;
In
water; acetonitrile;
at 23 ℃;
for 13h;
With
potassium hydrogenphosphate trihydrate;
In
water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
1.2: 1.5 h / -78 - -10 °C
1.3: pH 7 / Aqueous potassium phosphate buffer
2.1: hydrogen fluoride / acetonitrile; water / 13 h / 23 °C
With
N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; lithium diisopropyl amide;
In
tetrahydrofuran; water; acetonitrile;
1.2: Michael-Claisen cyclization;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: silver trifluoroacetate / 1,4-dioxane; water / 13 h / 23 - 40 °C
2.1: triphenylphosphine; diethylazodicarboxylate / dichloromethane; toluene / 0.03 h / 23 °C
2.2: 2 h / 23 °C
3.1: lithium diisopropyl amide; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran / 0.75 h / -78 °C / Inert atmosphere
3.2: 1.5 h / -78 - -10 °C
3.3: pH 7 / Aqueous potassium phosphate buffer
4.1: hydrogen fluoride / acetonitrile; water / 13 h / 23 °C
With
N,N,N,N,-tetramethylethylenediamine; hydrogen fluoride; silver trifluoroacetate; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile;
3.2: Michael-Claisen cyclization;
