Technology Process of (3,5-dibenzyloxy-2-methyl-4-<(2)H3>methylphenyl)propanone
There total 6 articles about (3,5-dibenzyloxy-2-methyl-4-<(2)H3>methylphenyl)propanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
methanol;
at 25 ℃;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 63 percent / potassium carbonate / butan-2-one / 6 h / Heating
2: 77 percent / lithium aluminium hydride / tetrahydrofuran / 0.25 h
3: 81 percent / phosphorous tribromide / diethyl ether / 0.08 h
4: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 5 min, 2.) 1 h
5: 65 percent / aq. H2SO4 / methanol / 0.17 h / 25 °C
With
lithium aluminium tetrahydride; sulfuric acid; phosphorus tribromide; potassium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; diethyl ether; butanone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 75 percent / diethyl ether / 0 °C
2: 63 percent / potassium carbonate / butan-2-one / 6 h / Heating
3: 77 percent / lithium aluminium hydride / tetrahydrofuran / 0.25 h
4: 81 percent / phosphorous tribromide / diethyl ether / 0.08 h
5: 1.) lithium di-isopropylamide / 1.) THF, -78 deg C, 5 min, 2.) 1 h
6: 65 percent / aq. H2SO4 / methanol / 0.17 h / 25 °C
With
lithium aluminium tetrahydride; sulfuric acid; phosphorus tribromide; potassium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; diethyl ether; butanone;
