methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

Base Information

Chemical Name:methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate
CAS No.:470473-73-5
Molecular Formula:C₃₀H₃₆N₂O₅
Molecular Weight:504.626
Hs Code.:

Synonyms:methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

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Chemical Property of methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

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Technology Process of methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

There total 3 articles about methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 172405-21-9
methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

: 470473-73-5
methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 470473-73-5
methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 1 h / -40 - -25 °C

2: 95 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(02)00527-6

Reference yield:

: N-(2-aminoethyl)glycine methyl ester hydrochloride

: 470473-73-5
methyl N-[2-(N-monomethoxytrityl)aminoethyl]-N-tert-butyloxycarbonyl glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / triethylamine / CH₂Cl₂ / 1 h / -40 - -25 °C

2: 95 percent / triethylamine / CH₂Cl₂ / 5 h / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(02)00527-6