(S)-4-citronellyloxybenzoic acid

Base Information

• Chemical Name: (S)-4-citronellyloxybenzoic acid
• CAS No.: 144289-83-8
• Molecular Formula: C₁₇H₂₄O₃
• Molecular Weight: 276.376
• Mol file: 144289-83-8.mol

Synonyms:(S)-4-citronellyloxybenzoic acid

Chemical Property of (S)-4-citronellyloxybenzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-4-citronellyloxybenzoic acid

There total 3 articles about (S)-4-citronellyloxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C19H28O3 → (S)-4-citronellyloxybenzoic acid (144289-83-8)

Guidance literature:

With sodium hydroxide; In ethanol; for 3h; Reflux;

DOI:10.1016/j.molliq.2015.12.070

Reference yield:

Ethyl 4-hydroxybenzoate (120-47-8) → (S)-4-citronellyloxybenzoic acid (144289-83-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / Reflux; Inert atmosphere

2: sodium hydroxide / ethanol / 3 h / Reflux

With potassium carbonate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.molliq.2015.12.070

Reference yield:

(S)-3,7-dimethyl-6-octenyl tosylate (41144-01-8,67214-54-4,93303-23-2,116661-43-9) → (S)-4-citronellyloxybenzoic acid (144289-83-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / Reflux; Inert atmosphere

2: sodium hydroxide / ethanol / 3 h / Reflux

With potassium carbonate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.molliq.2015.12.070

upstream raw materials:

Ethyl 4-hydroxybenzoate

(S)-3,7-dimethyl-6-octenyl tosylate

Downstream raw materials:

C₆₈H₈₈O₁₂Si₃

C₂₄H₂₈O₄