(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Base Information

Chemical Name:(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate
CAS No.:1257657-43-4
Molecular Formula:C₃₇H₄₁N₃O₇S
Molecular Weight:671.814
Hs Code.:

Synonyms:(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

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Chemical Property of (S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

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Technology Process of (S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

There total 1 articles about (S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1257657-18-3
(S)-2-allyloxyoctanedioic acid 8-methyl ester

: 1257657-63-8
2-{[2-allyl-1-(toluene-4-sulfonyl)-1H-indole-3-carbonyl]-amino}-phenyl-ammonium chloride

: 1257657-43-4
(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: (S)-2-allyloxyoctanedioic acid 8-methyl ester; With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; for 0.25h; Cooling with ice; Inert atmosphere;

2-{[2-allyl-1-(toluene-4-sulfonyl)-1H-indole-3-carbonyl]-amino}-phenyl-ammonium chloride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm101092u

Reference yield: 72.0%

: 1257657-43-4
(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

: 1257657-44-5
(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: (S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate; Hoveyda-Grubbs catalyst second generation; In 1,2-dichloro-ethane; for 18h; Reflux;

With hydrogen; 3% Pd/C; In methanol; at 20 ℃; for 5h; under 760.051 Torr;

Reference yield:

: 1257657-43-4
(S)-methyl 3-(2-(2-allyl-1-tosyl-1H-indole-3-carboxamido)phenylcarbamoyl)-3-(allyloxy)propanoate

: 1257657-64-9
C₃₅H₃₇N₃O₇S

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In 1,2-dichloro-ethane; for 18h; Reflux; Inert atmosphere;
DOI:10.1021/jm101092u