N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

Base Information

Chemical Name:N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine
CAS No.:937725-66-1
Molecular Formula:C₃₃H₄₇F₃N₂OS
Molecular Weight:576.81
Hs Code.:

Synonyms:N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

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Chemical Property of N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

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Technology Process of N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

There total 5 articles about N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 937725-71-8
1,2,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)aniline

: 61204-01-1,62788-05-0
4-(trans-4-pentylcyclohexyl)benzonitrile

: 937725-66-1
N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

Guidance literature:: With methanesulfonic acid; at 150 ℃; for 0.5h;
DOI:10.1021/jo070122a

Reference yield:

: 937725-73-0
2,3,5,6-tetrafluoro-4-hexyloxynitrobenzene

: 937725-66-1
N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaOH / ethanol / 0.75 h / 0 °C

2: 91 percent / Fe; acetic acid / H₂O / 0.5 h / 100 °C

3: 76 percent / methanesulfonic acid / 0.5 h / 150 °C

With sodium hydroxide; methanesulfonic acid; iron; acetic acid; In ethanol; water;
DOI:10.1021/jo070122a

Reference yield:

: 937725-74-1
3,5,6-trifluoro-4-hexyloxy-1-nitro-2-(propylsulfanyl)benzene

: 937725-66-1
N-(2,3,5-trifluoro-4-hexyloxy-6-(propylsulfanyl)phenyl)-4-(4E-pentylcyclohexyl)benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Fe; acetic acid / H₂O / 0.5 h / 100 °C

2: 76 percent / methanesulfonic acid / 0.5 h / 150 °C

With methanesulfonic acid; iron; acetic acid; In water;
DOI:10.1021/jo070122a