Technology Process of C25H44OSi2
There total 4 articles about C25H44OSi2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/ja209553f
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere
2: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene / 17 h / 80 °C / Inert atmosphere
3: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
1H-imidazole; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1021/ja209553f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C / Inert atmosphere
1.2: 5 h / -78 - 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C / Inert atmosphere
3.1: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / 5,5-dimethyl-1,3-cyclohexadiene / 17 h / 80 °C / Inert atmosphere
4.1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
With
1H-imidazole; n-butyllithium; platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; hexane;
DOI:10.1021/ja209553f
