3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

Base Information

Chemical Name:3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate
CAS No.:205369-90-0
Molecular Formula:C₁₇H₂₄Cl₂N₃O₇P
Molecular Weight:484.273
Hs Code.:

Synonyms:3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

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Chemical Property of 3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

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Technology Process of 3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

There total 3 articles about 3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 205369-90-0
3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / stannous fluoride / dimethylformamide

2: 1.) NaOH / 1.) methanol, room temperature, 15 h, 2.) methanol, reflux, 15 h

With stannous fluoride; sodium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1021/jo961861m

Reference yield:

: 4-hydroxy-2-(1-hydroxy-3-butenyl)-1-nitrobenzene

: 205369-90-0
3-butenyl-1-{5-[(carbomethoxy)methoxy]-2-nitrophenyl} 1-N,N-bis(2-chloroethyl)phosphorodiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOH / 1.) methanol, room temperature, 15 h, 2.) methanol, reflux, 15 h

With sodium hydroxide;
DOI:10.1021/jo961861m