4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

Base Information

Chemical Name:4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene
CAS No.:870836-64-9
Molecular Formula:C₂₅H₂₄N₆O₄
Molecular Weight:472.503
Hs Code.:

Synonyms:4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

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Chemical Property of 4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

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Technology Process of 4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

There total 2 articles about 4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 4-(N-methyl-N-(2-hydroxyethyl)amino)-4'-(4-nitrophenylazo)azobenzene

: 920-46-7,26937-45-1
Methacryloyl chloride

: 870836-64-9
4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ma051455h

Reference yield:

: 93-90-3
N-(2-hydroxyethyl)-N-methylaminobenzene

: 870836-64-9
4-{(2-methacryloyloxyethyl)methylamino}-4'-(4-nitrophenylazo)azobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: conc. HCl; aq. NaNO₂ / dimethylformamide / 2 h / 0 °C

1.2: 56 percent / acetic acid / dimethylformamide / 20 h / 0 - 20 °C

2.1: 69 percent / Et₃N / tetrahydrofuran / 0 - 20 °C

With hydrogenchloride; triethylamine; sodium nitrite; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ma051455h