Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Base Information

Chemical Name:Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside
CAS No.:130450-79-2
Molecular Formula:C₁₇H₂₄O₅S
Molecular Weight:340.441
Hs Code.:

Synonyms:Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Suppliers and Price of Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Chemical Property:

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Technology Process of Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

There total 4 articles about Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2595-43-9,185549-85-3
Methyl 2,3,4-tri-O-acetyl-1-thio-β-D-xylopyranoside

: 130450-79-2
Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / NaOMe / methanol / 1 h / Ambient temperature

2: 70 percent / 5M HCl / dimethylformamide; methanol / 0.5 h / 5 °C

3: 1.)NaH / 1.)DMF, r.t., 2.)r.t.

With hydrogenchloride; sodium methylate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M

Reference yield:

: 2595-45-1
Methyl 1-thio-β-D-xylopyranoside

: 130450-79-2
Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 5M HCl / dimethylformamide; methanol / 0.5 h / 5 °C

2: 1.)NaH / 1.)DMF, r.t., 2.)r.t.

With hydrogenchloride; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M

Reference yield:

: 4049-33-6
tetra-O-acetyl-β-D-xylopyranose

: 130450-79-2
Methyl 2,3-O-isopropylidene-4-O-(p-methoxybenzyl)-1-thio-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 38 percent / SnCl₄ / 1,2-dichloro-ethane / 3 h / Ambient temperature

2: 92 percent / NaOMe / methanol / 1 h / Ambient temperature

3: 70 percent / 5M HCl / dimethylformamide; methanol / 0.5 h / 5 °C

4: 1.)NaH / 1.)DMF, r.t., 2.)r.t.

With hydrogenchloride; sodium methylate; tin(IV) chloride; sodium hydride; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84242-M