1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

Base Information

Chemical Name:1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole
CAS No.:119935-46-5
Molecular Formula:C₁₉H₁₈N₂O₅S
Molecular Weight:386.428
Hs Code.:

Synonyms:1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

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Technology Process of 1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

There total 2 articles about 1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 108-98-5
thiophenol

: 119935-41-0
1-Methyl-2-bromomethyl-3-ethoxycarbonyl-5-acetoxy-6-nitroindole

: 119935-46-5
1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

Guidance literature:: With potassium hydroxide; In ethanol; 1.) room temp., 1 h, 2.) water bath, 2 h;
DOI:10.1007/BF00771642

Reference yield:

: 52580-53-7
5-acetoxy-1,2-dimethyl-6-nitro-1H-indole-3-carboxylic acid ethyl ester

: 119935-46-5
1-Methyl-2-phenylthiomethyl-3-ethoxycarbonyl-5-oxy-6-nitroindole

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / NBS, benzoyl peroxide / CCl₄ / 4 h / Heating; Irradiation

2: 79 percent / KOH / ethanol / 1.) room temp., 1 h, 2.) water bath, 2 h

With potassium hydroxide; N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; ethanol;
DOI:10.1007/BF00771642